Gravimetric determination of pipette errors
ثبت نشده
چکیده
In chemical measurements (for instance in titrimetric analysis) it is very important to precisely measure amount of liquid, the measurement is performed with use of various measuring vessels. Presently laboratories use all kinds of glass measuring vessels like: beakers, flasks, etc., for measurement of bigger volumes of liquid, and in case of small volumes glass pipettes. Glass pipettes have been used for very precise measurements since the 70’s of 20 century. In 1964 during XII Measuring Conference, a measuring value of a “liter” from outside SI set has been accepted for official use. A liter [l] officially stands for a cubic decimeter [dm3]. In analytical chemistry, it is much more convenient to express volume in liters, and such is used in various documents, norms and publications. Development of science results in development in metrology of various sizes. Today one can observe even more precise and accurate measuring instruments. It is not different in case of measuring liquids with use of pipettes, commonly known as „liquid handling”. Presently, laboratory operators use modern pipettes, which can dose volumes like tenth of microliter [ul].
منابع مشابه
GRAVIMETRIC DETERMINATION OF NICKEL WITH CYCLOHEXYLIDINE-AMMONIUM-2-AMINOC YCLOHEXY LIDINE- 1-CYCLOHEXENE-1-DITHIOCARBOXYLATE
Cyclohexylidine-ammonium-2-aminocyclohexyline-l-cyclohexee-l- dithiocarboxylate (CCCD) is employed for the gravimetric determination of Ni (II). In neutral or ammoniacal solutions, the metal forms a violet precipitate with the reagent which can be weighed as Ni (C13H18NS2)a2f ter drying at 115 - 120?C Using this procedure, the nickel content of steel samples can also be determined accurate...
متن کاملComparison of gravimetric and gas chromatographic methods for assessing performance of textile materials against liquid pesticide penetration.
Penetration of liquid pesticides through textile materials is a criterion for determining the performance of protective clothing used by pesticide handlers. The pipette method is frequently used to apply liquid pesticides onto textile materials to measure penetration. Typically, analytical techniques such as Gas Chromatography (GC) are used to measure percentage penetration. These techniques ar...
متن کاملMean kernels to improve gravimetric geoid determination based on modified Stokes's integration
Gravimetric geoid computation is often based on modified Stokes’s integration, where Stokes’s integral is evaluated with some stochastic or deterministic kernel modification. Accurate numerical evaluation of Stokes’s integral requires the modified kernel to be integrated across the area of each discretised grid cell (mean kernel). Evaluating the modified kernel at the centre of the cell (point ...
متن کاملINTRACYTOPLASMIC SPERM INJECTION (lCSI) IN MICE BY A NEW HOLDING PIPETTE
Mice are ideal models for ICSI experiments because of the ease of culturing eggs/embryos in vitro and the availability of ample genetic information. Unfortunately, it has been extremely difficult. In this study we improved the mouse ICSI method by using a new holding pipette that was made of two pipettes such that one pipette was pulled and heat merged into the other one. The outer pipette ...
متن کاملGravimetric and Spectrophotometric Methods for the Determination of Piperazine. Picrolonic vs. Picric Acid
In the present work two new analytical methods, a gravimetric and a spectrophotometric, for the assay of piperazine free base and its soluble salts in the anthelmitic preparation "Oxyuran", are described. Both approaches are based on the quantitative reaction between the diprotonated cationic form of piperazine and the 3-methyl-4-nitro-1-p-nitrophenyl-5-pyrazolone (picrolonic acid), in sulfuric...
متن کامل